| Individual course details | ||||||||||
| Study programme | Applied and computational physics | |||||||||
| Chosen research area (module) | Metrology/computational physics | |||||||||
| Nature and level of studies | ||||||||||
| Name of the course | Mass spectrometry and physics of vacuum | |||||||||
| Professor (lectures) | Ivan Belča | |||||||||
| Professor/associate (examples/practical) | ||||||||||
| Professor/associate (additional) | Miloš Vićić | |||||||||
| ECTS | Status (required/elective) | |||||||||
| Access requirements | ||||||||||
| Aims of the course | Addoption of principles of mass spectrometry and physics of vacuum. | |||||||||
| Learning outcomes | Knowledge in vacuum physics and technics as well as ability for practical work with mass spectrometer and mass spectra analisys. | |||||||||
| Contents of the course | ||||||||||
| Lectures | Roots of mass spectrometry. What is mass spectrometer. Characteristics of MS. Introduction of samples. Types of ionic sources. Plasma discharge. Chemical ionization. Electrospray ionization. Fast atom bombardment. Field ionization.Laser ionization. MALDI. Analizers. Magnetic and electrostatic sectors. Quadrupol mass filter, quadrupol mass trap. GT-ICR, TOF. Tandem mass spectrometry. Ion detector, electrom multipliers. Application of MS in strustural analisys. Quantitative analisys. Isotope ratio. Molecular mass determination. Interpretation of mass spectra. Vacuum and systems: basic quantities. Vacuum pumps. Low presure measurement. | |||||||||
| Examples/ practical classes | exercises on quadrupol mass spectrometer and analisys of know unknown spectra. | |||||||||
| Recommended books | ||||||||||
| 1 | Interpretation of mass spectra, F.W.McLafferty and F.Tureček; | |||||||||
| 2 | М. Курепа, Б. Чобић, Физика и техника вакуума | |||||||||
| 3 | ||||||||||
| 4 | ||||||||||
| 5 | ||||||||||
| Number of classes (weekly) | ||||||||||
| Lectures | Examples&practicals | Student project | Additional | |||||||
| Teaching and learning methods | Theoretical lessons, seminars, practical work. | |||||||||
| Assessment (maximal 100) | ||||||||||
| assesed coursework | mark | examination | mark | |||||||
| coursework | written examination | |||||||||
| practicals | oral examination | |||||||||
| papers | ||||||||||
| presentations | ||||||||||